Spectroscopic Methods for Nanomaterials Characterization

Front Cover
Sabu Thomas, Raju Thomas, Ajesh K Zachariah, Raghvendra Kumar Mishra
Elsevier, May 19, 2017 - Technology & Engineering - 444 pages

Nanomaterials Characterization Techniques, Volume Two, part of an ongoing series, offers a detailed analysis of the different types of spectroscopic methods currently being used in nanocharacterization. These include, for example, the Raman spectroscopic method for the characterization of carbon nanotubes (CNTs).

This book outlines the different kinds of spectroscopic tools being used for the characterization of nanomaterials and discusses under what conditions each should be used. The book is intended to cover all the major spectroscopic techniques for nanocharacterization, making it an important resource for both the academic community at the research level and the industrial community involved in nanomanufacturing.

  • Explores how spectroscopy and X-ray-based nanocharacterization techniques are applied in modern industry
  • Analyzes all the major spectroscopy and X-ray-based nanocharacterization techniques, allowing the reader to choose the best for their situation
  • Presents a method-orientated approach that explains how to successfully use each technique
 

Contents

A Facile Approach for the Characterization of Nanomaterials
55
4 Fourier Transform Infrared Spectroscopy
73
5 Raman Spectroscopy
95
6 HighVacuum TipEnhanced Raman Spectroscopy
129
7 Confocal Raman Spectroscopy
141
8 Inductively Coupled Plasma Mass Spectrometry
163
9 Electromagnetic Characterization of Materials by Vector Network Analyzer Experimental Setup
195
10 Dielectric Spectroscopy
237
11 Dielectric and Magnetic Loss Behavior of Nanooxides
301
Basic Principles and Practical Guide to Exotic Mössbauer Isotopes
321
13 Nuclear Magnetic Resonance Spectroscopy
369
Index
417
Back Cover
425
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About the author (2017)

Professor Sabu Thomas is the Director of Centre for Nanoscience and Nanotechnology, Mahatma Gandhi University, Kottayam, Kerala, India. He is also currently the Chairman of the Trivandrum Engineering Science and Technology Research Park (TrESPARK), Trivandrum, Kerala, India. He was the former Vice Chancellor of Mahatma Gandhi University, Kottayam, Kerala, India. Prof. Thomas is a highly committed teacher and a remarkably active researcher well-known nationally and internationally for his outstanding contributions in polymer science and nanotechnology. He has published over 1400 research articles in international refereed journals. and has also edited and written 210 books. His H-index is 140 and total citations are more than 94,000. He has supervised 125 PhD theses. He has received many international and national awards and recognitions. Under the leadership of Prof. Thomas, Mahatma Gandhi University has been transformed into a top University in India.

Prof (Dr). Raju Thomas is currently Vice Chancellor of Middle East University FZE, P.O. BOX 37173, Al Hamara, Ras Al Khaimah, and United Arab Emirates. Dr. Thomas started Professorship from Research and Postgraduate Department of Chemistry, Mar Thoma College, Tiruvalla-3, Kerala, India. Dr. Thomas procured Ph.D degree under the supervision of Prof. (Dr). Sabu Thomas, Director of International and Interuniversity Centre for Nanoscience and Nanotechnology, Mahatma Gandhi University, Kottayam, Kerala, India. He has extensive research experience in Nanoscience and Nanotechnology. He has twelve years of research experience in the Organic Chemistry and Polymer Chemistry laboratories of the School of Chemical Sciences, Mahatma Gandhi University, Kottayam, Kerala, India. He has also worked in the laboratory of Applied Rheology and Polymer processing of Katholieke University, Leuven, Belgium and in the laboratory at Leibniz Institute of Polymer Research Dresden, Germany. He has widely studied the kinetics of curing, morphology developments and structural characteristics of in-situ cured nanocomposites based on epoxy resin and reactive rubbers. His research is reflected in his six published research articles in international journals and additional articles which are currently under review. In addition, many articles are published in popular journals. He has co-authored many chapters and co-editor of a book entitled “Micro and Nanostructured Epoxy/Rubber Blends” which was recently published by Wiley and Sons. He has attended many national and international seminars/ conferences and presented many research papers. He is an approved research guide in Chemistry of Mahatma Gandhi University, Kottayam, India and has availed projects from University Grants Commission (UGC), Department of Science and Technology- Science and Engineering Research Board (DST-SERB) and Kerala Science Council for Science, Technology and Environment (KSCSTE).

Prof. Ajesh K. Zachariah is currently working as Assistant Professor in the Department of Chemistry, Mar Thoma College, Tiruvalla. He had done Doctoral Research in Polymer Chemistry at School of Chemical Sciences, Mahatma Gandhi University, Kottayam, Kerala, India. He has ten years’ research experience in nanomaterials and characterization. Expert in sophisticated analytical techniques such as Atomic Force Microscopy (AFM), X ray diffraction Technique (XRD), Gas Permeability Tester, Dynamic Mechanical Analyser (DMA), Rubber Process Analyser (RPA)and Oscillating Disc Rheometer (ODR). Published nine internationally cited articles, two international books and applied one Indian patent. He presented articles in different national and international conferences. He bagged Young Technological Innovation (GYTI) Award 2013, the meritorious research scholar award from UGC, India in 2009 and young researcher award in Nanosat-2010. His research areas are nanomaterial, naocomposites, elastomer-elastomer blend systems, sensors, membranes, computational chemistry and environmental chemistry.

Raghvendra Kumar Mishra is a researcher with Cranfield University, United Kingdom. His research interests focus on nanomaterials and polymer composites, including new applications of nanomaterials, developing nanomaterials-based systems for diverse functionalities, creating biopolymer-based composites, and utilizing advanced fabrication techniques such as electrospinning and 3D printing.

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